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The MRSEC Facilities Network is a nationwide partnership of NSF supported MRSEC centers designed to provide support to researchers in the broad area of Materials Research in academic, government and industrial laboratories around the world.
The Bruker-AXS Microdiffractometer

The Bruker-AXS Microdiffractometer

Description

Wide-angle X-ray scattering is used to study structural characteristics and to identify powders, thin films, and crystals.
Microdiffraction can be used for x-ray analysis of very small samples or small areas of larger samples. The x-ray beam can be collimated down to a 50 micron spot size. A video-microscope and laser pointer allows for the beam's precise positioning. The multi-wire two-dimensional area detector allows for quick data acquisition and orientation information. This detector, combined with the 1/4 circle Eulerian cradle sample holder is perfect for pole figure (texture) analysis.

Equipment

  • Bruker-AXS Microdiffractometer with 2.2 kW Sealed Cu X-ray Source
  • Incident Beam Monochromater
  • 1/4 circle Eulerian Cradle Sample Holder
  • Hi-Star 2-D Area Detector
  • Temperature Control (-20° to 200° C)
  • Optional Chromium X-Ray Source

Applications

  • Phase identification
  • Thin-film analysis
  • Lattice parameter determination
  • Purity/quality control of materials
  • Determination of crystallinity of polycrystalline materials
  • Stress analysis
  • Orientation of single crystals
  • Particle size determination
  • Pole figure (texture) analysis

Specifications

Samples can be analyzed in bulk, powder, thin film and solution form.

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